2-氯-1,3-二甲基咪唑六氟磷酸盐合成路线 （共 5 条）
反应条件
KPF6 in acetonitrile T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Kitamura, Mitsuru; Kato, So; Yano, Masakazu; Tashiro, Norifumi; Shiratake, Yuichiro; Sando, Mitsuyoshi; Okauchi, Tatsuo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 25 p. 4397 - 4406
反应条件
KPF6 Substitution; deoxygenation;
参考文献
Organic Letters, , vol. 2, # 23 p. 3539 - 3542
反应条件
KPF6; oxalyl dichloride; water 1.) CH2Cl2, reflux, 3 h, 2.) CH2Cl2, 0 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Organic Preparations and Procedures International, , vol. 30, # 4 p. 477 - 481
反应条件
sodium azide in acetonitrile T=0°C; 0.5 h;
参考文献
Kitamura, Mitsuru; Kato, So; Yano, Masakazu; Tashiro, Norifumi; Shiratake, Yuichiro; Sando, Mitsuyoshi; Okauchi, Tatsuo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 25 p. 4397 - 4406
反应条件
in 1,2-dichloro-ethane
T=60°C; 72 h;
参考文献
F. HOFFMANN-LA ROCHE AG
Patent: WO2005/5397 A1, 2005 ;
Location in patent: Page/Page column 71-72 ;
WO 2005/005397 A1
