2-(1H-吡唑-1-基)乙胺合成路线 （共 6 条）
反应条件
hydrazine in ethanol T=20°C; 6 h; Heating / reflux;
参考文献
APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
Patent: WO2005/26159 A1, 2005 ;
Location in patent: Page/Page column 37 ;
反应条件
hydrogen; palladium 10 on activated carbon in ethanol T=20°C; P=760.051 Torr; 1 h;
参考文献
WO2004/39795 A2, ;
Page 160 ;
WO 2004/039795 A2
反应条件
1: [3,2-c]pyrazole With sodium hydroxide in acetonitrile T=20°C; 0.5 h; 2: 1-chloro-2-aminoethane in acetonitrile T=75°C; 5.5 h;
参考文献
Hamann, Jessica Nadine; Tuczek, Felix
Chemical Communications, 2014 , vol. 50, # 18 p. 2298 - 2300
反应条件
1: 89 percent / acetonitrile / 72 h / Heating 2: 62 percent / hydrazine monohydrate / methanol / 3 h / Heating View Scheme
参考文献
Dalton Transactions, , # 47 p. 5630 - 5640
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 19, p. 1428,1431
反应条件
1: ethanolic NH3 2: LiAlH4; diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 19, p. 1428,1431
