3-[2-(2-羟基乙氧基)乙氧基]丙腈合成路线 (共 13 条)
反应条件
sodium hydroxide 1) benzene, 70 to 80 deg C.; Yield given. Multistep reaction;
参考文献
Movsumzade, E. M.; Rasulbekova, T. I.; Kulieva, D. A.; Aliev, G. R.; Movsumzade, S. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 11 p. 2132 - 2135
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 11 p. 2334 - 2337
参考文献
Maeshima
Kogyo Kagaku Zasshi, 1959 , vol. 62, p. 1849,1850
Chem.Abstr., 1962 , vol. 57, p. 16863
参考文献
Union Carbide Corp.
Patent: US2853510 , 1956 ;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 3; 4 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in tert-butyl methyl ether T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in methanol T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt T=125°C; P=47304.6 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in water T=60°C; P=42133 Torr; 4 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 3; 6 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in tert-butyl methyl ether T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4-5; 7 ;
反应条件
hydrogen; Grace 2724 sponge cobalt in methanol T=120°C; P=42133 Torr; 5 h; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1512675 A1, 2005 ;
Location in patent: Page/Page column 4; 7 ;