1.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C / |Inert atmosphere
1.2: 5 h / 20 °C / |Inert atmosphere
2.1: dichloro(2-pyridinecarboxylato)gold / dichloromethane / 1 h / 0 °C
View Scheme
参考文献
McGonigal, Paul R.; De Leon, Claudia; Wang, Yahui; Homs, Anna; Solorio-Alvarado, Cesar R.; Echavarren, Antonio M.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 52 p. 13093 - 13096
1: phenylmethylacetylene With n-butyllithium
2: methyl chloroformate
参考文献
Covarrubias-Zuniga, Adrian; San German-Sanchez, Laura; Maldonado, Luis A.; Romero-Ortega, Moises; Avila-Zarraga, Jose G.
Synthesis, 2005 , # 14 art. no. M06404SS, p. 2293 - 2296