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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-(苄氧基)己醛
合成路线
（共 13 条）
71126-73-3
6-(苄氧基)-1-己醇
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1: With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-78°C; 0.5 h; Inert atmosphere; 2: With triethylamine in dichloromethane T=-78 - 0°C; 0.5 h; Inert atmosphere;
参考文献
Sudhakar, Gangarajula; Reddy, Karla Janardhan; Nanubolu, Jagadeesh Babu
Tetrahedron, 2013 , vol. 69, # 11 p. 2419 - 2429
629-11-8
1,6-己二醇
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1.1: sodium hydride / dimethylformamide / 0.17 h / -10 °C 1.2: 47 percent / dimethylformamide / 3.5 h / 20 °C 2.1: 66 percent / oxalyl chloride; triethylamine; DMSO / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Chang, Meng-Yang; Chen, Chung-Yi; Chen, Shui-Tein; Chang, Nein-Chen
Tetrahedron, 2003 , vol. 59, # 38 p. 7547 - 7553
100-39-0
溴化苄
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil 2: pyridinium chlorochromate / dichloromethane View Scheme
参考文献
Hamilton, Lynne; Stevenson, M. Hilary; Boyd, Derek R.; Brannigan, Ian N.; Treacy, Alan B.; Hamilton, John T. G.; McRoberts, W. Colin; Elliott, Christopher T.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 2 p. 139 - 146
148840-81-7
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
toluene-4-sulfonic acid in tetrahydrofuran; water; isopropyl alcohol 1 h; Heating;
参考文献
Boden; Chambers; Stevens
Synthesis, 1993 , # 4 p. 411 - 420
18751-83-2
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1: 1) NaH / 1) DMF, 5 to 20 deg C, 1 h, 2) 5-10 deg C, 30 min 2: 96 percent / p-TsOH / tetrahydrofuran; H2O; propan-2-ol / 1 h / Heating View Scheme
参考文献
Boden; Chambers; Stevens
Synthesis, 1993 , # 4 p. 411 - 420
100-44-7
苄基氯
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1.1: sodium hydride / tetrahydrofuran / 2 h / Reflux 1.2: 20 °C 2.1: tetrabutylammomium bromide; sodium acetate; pyridinium chlorochromate / dichloromethane / 2 h / 20 °C / Molecular sieve View Scheme
参考文献
Pan, Xiangcheng; Lacote, Emmanuel; Lalevee, Jacques; Curran, Dennis P.
Journal of the American Chemical Society, 2012 , vol. 134, # 12 p. 5669 - 5674
4286-55-9
6-溴正己醇
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C 2: silica gel; pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Yu, Wenquan; Gill, Tina; Wang, Lijuan; Du, Yanming; Ye, Hong; Qu, Xiaowang; Guo, Ju-Tao; Cuconati, Andrea; Zhao, Kang; Block, Timothy M.; Xu, Xiaodong; Chang, Jinhong
Journal of Medicinal Chemistry, 2012 , vol. 55, # 13 p. 6061 - 6075
100-51-6
苯甲醇
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C 2: silica gel; pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Yu, Wenquan; Gill, Tina; Wang, Lijuan; Du, Yanming; Ye, Hong; Qu, Xiaowang; Guo, Ju-Tao; Cuconati, Andrea; Zhao, Kang; Block, Timothy M.; Xu, Xiaodong; Chang, Jinhong
Journal of Medicinal Chemistry, 2012 , vol. 55, # 13 p. 6061 - 6075
7356-06-1
6,6-二乙氧基己氧基甲基苯
→
反应条件
101492-91-5
6-(苄氧基)己醛
反应条件
hydrogenchloride
参考文献
Perrine
Journal of Organic Chemistry, 1953 , vol. 18, p. 1356,1361
101492-91-5
6-(苄氧基)己醛
→
反应条件
129648-96-0
钠3-[4-[(4-氯苯基)磺酰基氨基]丁基]-6-丙-2-基薁e-1-磺酸酯
反应条件
1: morpholine 2: AlCl3, anisole 3: pyridine 4: NaH 5: 100percent phosphoric acid 6: 1.) SO3Py, 2.) MeONa / 2.) MeOH View Scheme
参考文献
Tomiyama, Tsuyoshi; Wakabayashi, Shuichi; Kosakai, Kazuhiro; Yokota, Masayuki
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2323 - 2326
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