反应条件
air in ethanol suspn. of HS2PPh2 in EtOH added to suspn. of Sn compd. in EtOH; stirredfor 15 min; suspn. of semicarbazone ligand (molar ratio 1:1:1) in EtOH added; stirred for 7 d; filtered; soln. stored at 0°C; filtered; solid vac. dried (dithiophosphinato complex); remaining mother liquor concd. in air (monothiophosphinato complex); elem. anal.;
参考文献
Casas, Jose S.; Castineiras, Alfonso; Rodriguez-Argiielles, Maria C.; Sanchez, Agustin; Sordo, Jose; Vazquez-Lopez, Antonia; Vazquez-Lopez, Ezequiel M.
Journal of the Chemical Society, Dalton Transactions, 2000 , # 22 p. 4056 - 4063
