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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
10152-41-7
合成路线
（共 18 条）
127-08-2
乙酸钾
+
83526-50-5
→
反应条件
10152-41-7
反应条件
in dimethyl sulfoxide T=140°C; 0.5 h;
参考文献
Hirth; Barner
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 1059 - 1084
83526-53-8
→
反应条件
10152-41-7
反应条件
1: dimethylformamide / 80 °C 2: pyridine / CHCl3 / Ambient temperature 3: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature 4: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature 5: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 6: 78 percent / pyridine / CH2Cl2 / 50 °C 7: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Hirth; Barner
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 1059 - 1084
83526-57-2
→
反应条件
10152-41-7
反应条件
1: pyridine / CHCl3 / Ambient temperature 2: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature 3: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature 4: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 5: 78 percent / pyridine / CH2Cl2 / 50 °C 6: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Hirth; Barner
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 1059 - 1084
83526-54-9
→
反应条件
10152-41-7
反应条件
1: toluene / 1 h / 80 °C 2: pyridine / CHCl3 / Ambient temperature 3: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature 4: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature 5: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 6: 78 percent / pyridine / CH2Cl2 / 50 °C 7: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Hirth; Barner
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 1059 - 1084
83526-60-7
→
反应条件
10152-41-7
反应条件
1: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature 2: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature 3: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 4: 78 percent / pyridine / CH2Cl2 / 50 °C 5: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Hirth; Barner
Helvetica Chimica Acta, 1982 , vol. 65, # 3 p. 1059 - 1084
10567-22-3
→
反应条件
10152-41-7
反应条件
1: 78 percent / pyridine / CH2Cl2 / 50 °C 2: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Takano; Akiyama; Ogasawara
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 2 p. 791 - 794
10585-86-1
→
反应条件
10152-41-7
反应条件
1: 81.5 percent / 1N HCl / dioxane / 1 h / Heating 2: 78 percent / pyridine / CH2Cl2 / 50 °C 3: 81.5 percent / dimethylsulfoxide / 0.5 h / 140 °C View Scheme
参考文献
Takano; Akiyama; Ogasawara
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 2 p. 791 - 794
108-05-4
醋酸乙烯酯
+
544-62-7
鲨肝醇
→
反应条件
10152-41-7
+
18330-40-0
+
83526-72-1
+
83526-75-4
反应条件
pseudomonas fluorescens lipase in chloroform T=20°C; 72 h; Title compound not separated from byproducts;
参考文献
Halldorsson, Arnar; Thordarson, Pall; Kristinsson, Bjorn; Magnusson, Carlos D.; Haraldsson, Gudmundur G.
Tetrahedron Asymmetry, 2004 , vol. 15, # 18 p. 2893 - 2899
112-89-0
1-溴十八烷
→
反应条件
10152-41-7
反应条件
1: tetrabutylammonium bromide; potassium hydroxide / 18 h / 35 - 40 °C 2: 903 mg / p-toluenesulfonic acid / tetrahydrofuran; H2O / Heating 3: Pseudomonas fluorescens lipase / CHCl3 / 72 h / 20 °C View Scheme
参考文献
Halldorsson, Arnar; Thordarson, Pall; Kristinsson, Bjorn; Magnusson, Carlos D.; Haraldsson, Gudmundur G.
Tetrahedron Asymmetry, 2004 , vol. 15, # 18 p. 2893 - 2899
16725-43-2
→
反应条件
10152-41-7
反应条件
1: 903 mg / p-toluenesulfonic acid / tetrahydrofuran; H2O / Heating 2: Pseudomonas fluorescens lipase / CHCl3 / 72 h / 20 °C View Scheme
参考文献
Halldorsson, Arnar; Thordarson, Pall; Kristinsson, Bjorn; Magnusson, Carlos D.; Haraldsson, Gudmundur G.
Tetrahedron Asymmetry, 2004 , vol. 15, # 18 p. 2893 - 2899
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