4,6-二溴噻吩并[3,4-c]呋喃-1,3-二酮合成路线 (共 4 条)
反应条件
acetic anhydride Inert atmosphere;
参考文献
Cabanetos, Clement; El Labban, Abdulrahman; Bartelt, Jonathan A.; Douglas, Jessica D.; Mateker, William R.; Frechet, Jean M. J.; McGehee, Michael D.; Beaujuge, Pierre M.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4656 - 4659
反应条件
1: acetic acid; bromine / |Inert atmosphere 2: acetic anhydride / |Inert atmosphere View Scheme
参考文献
Cabanetos, Clement; El Labban, Abdulrahman; Bartelt, Jonathan A.; Douglas, Jessica D.; Mateker, William R.; Frechet, Jean M. J.; McGehee, Michael D.; Beaujuge, Pierre M.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4656 - 4659
反应条件
1: in tetrahydrofuran T=50°C; 3 h; Inert atmosphere; 2: With thionyl chloride in tetrahydrofuran T=55°C; 4 h; Inert atmosphere;
参考文献
Cabanetos, Clement; El Labban, Abdulrahman; Bartelt, Jonathan A.; Douglas, Jessica D.; Mateker, William R.; Frechet, Jean M. J.; McGehee, Michael D.; Beaujuge, Pierre M.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4656 - 4659
反应条件
1: in tetrahydrofuran
T=50°C; 3 h; Inert atmosphere;
2: With thionyl chloride in tetrahydrofuran
T=55°C; 4 h; Inert atmosphere;
参考文献
Cabanetos, Clement; El Labban, Abdulrahman; Bartelt, Jonathan A.; Douglas, Jessica D.; Mateker, William R.; Frechet, Jean M. J.; McGehee, Michael D.; Beaujuge, Pierre M.
Journal of the American Chemical Society, 2013 , vol. 135, # 12 p. 4656 - 4659