(甲氧基-苯基甲基)苯合成路线 （共 143 条）
反应条件
methanol
T=100 - 105°C;
参考文献
Sommelet
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1922 , vol. 175, p. 1151
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1925 , vol. 180, p. 78
反应条件
para-dicyanobenzene in methanol; acetonitrile
T=80°C; Irradiationother triarylalkanes; Product distributionMechanism;
参考文献
Popielarz; Arnold
Journal of the American Chemical Society, 1990 , vol. 112, # 8 p. 3068 - 3082
反应条件
1: metallic potassium / tetrahydrofuran / 2.5 h / Ambient temperature
2: 1.) N,N,N-trimethylphenylammonium perchlorate; 2.) air / 1.) THF, room temp., 24 h; 2.) diethyl ether, water, -60 deg C - -50 deg C, 1h.
View Scheme
参考文献
Selivanov, B. A.; Bil'kis, I. I.; Danilov, I. S.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1888 - 1896
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2143 - 2152
反应条件
1: 2.) air / 1.) THF, room temp., 24 h; 2.) diethyl ether, water, -60 deg C - -50 deg C, 1h.
2: metallic potassium / tetrahydrofuran / 2.5 h / Ambient temperature
3: 1.) N,N,N-trimethylphenylammonium perchlorate; 2.) air / 1.) THF, room temp., 24 h; 2.) diethyl ether, water, -60 deg C - -50 deg C, 1h.
View Scheme
参考文献
Selivanov, B. A.; Bil'kis, I. I.; Danilov, I. S.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1888 - 1896
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2143 - 2152
反应条件
1: air / dichloromethane / 0.5 h / 0 °C / |Schlenk technique
2: dichloromethane / 20 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Goto, Akihiro; Otake, Kazuki; Kubo, Ozora; Sawama, Yoshinari; Maegawa, Tomohiro; Fujioka, Hiromichi
Chemistry - A European Journal, 2012 , vol. 18, # 36 p. 11423 - 11432
反应条件
λ: 288 nm.Photolysis; Quantum yield;
参考文献
Kirmse; Horner
Justus Liebigs Annalen der Chemie, 1959 , vol. 625, p. 34,40
反应条件
lithium chloride in N,N-dimethyl-formamide
(electrochemical reduction);
参考文献
Lund,H.; Simonet,J.
Bulletin de la Societe Chimique de France, 1973 , p. 1843 - 1849
反应条件
potassium tert-butylate in benzene
参考文献
Schaumann,E.; Grabley,F.-F.
Justus Liebigs Annalen der Chemie, 1977 , p. 88 - 100
参考文献
Bartlett,P.D. et al.
Journal of the American Chemical Society, 1969 , vol. 91, # 23 p. 6362 - 6366
反应条件
sodium carbonate in methanol
Irradiation;
参考文献
Sonawane, H. R.; Sethi, S. C.; Merchant, S. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 10 p. 940 - 943
