2-[(7-溴庚基)氧基]四氢-2H-吡喃合成路线 (共 23 条)
反应条件
n-butyllithium; toluene-4-sulfonic acid
1) hexane; 2) THF, hexane, HMPA, room temperature, 10 h; 3) methanol, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Martichonok, Valeri; Jones, J. Bryan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 22 p. 2927 - 2930
反应条件
(i) nBuLi, (ii) /BRN= 1237703/, (iii) aq. AcOH, THF; Multistep reaction;
参考文献
Narasaka,K. et al.
Chemistry Letters, 1977 , p. 959 - 962
反应条件
1: (i) nBuLi, (ii) /BRN= 1237703/, (iii) aq. AcOH, THF
2: (i) CrO3, Py, (ii) MCPBA, (iii) NaBH4
View Scheme
参考文献
Narasaka,K. et al.
Chemistry Letters, 1977 , p. 959 - 962