2-(羟乙氨基)-6-苄氨基-9-甲基嘌呤合成路线 （共 10 条）
反应条件
in N,N-dimethyl-formamide T=160°C; 2.5 h;
参考文献
Hocart, Charles H.; Letham, David S.; Parker, Charles W.
Phytochemistry (Elsevier), 1991 , vol. 30, # 8 p. 2477 - 2486
反应条件
sodium hydride in N,N-dimethyl acetamide 0.5 h;
参考文献
Nugiel; Cornelius; Corbett
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 201 - 203
反应条件
1: 89 percent / BOP; DBU / dimethylformamide; dimethylsulfoxide / 50 h / 20 - 60 °C 2: HOAc; NaBH3CN / methanol / 48 h / 20 °C 3: aq. HCl / methanol / 0.5 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 8, # 11 p. 2425 - 2428
反应条件
1: 89 percent / BOP; DBU / dimethylformamide; dimethylsulfoxide / 50 h / 20 - 60 °C 2: HOAc; NaBH3CN / methanol / 48 h / 20 °C 3: aq. HCl / methanol / 0.5 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 8, # 11 p. 2425 - 2428
反应条件
1: HOAc; NaBH3CN / methanol / 48 h / 20 °C 2: aq. HCl / methanol / 0.5 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 8, # 11 p. 2425 - 2428
反应条件
1: NaH / dimethylformamide 2: N-methylpyrrolidinone / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 21 p. 2697 - 2702
反应条件
1: butan-1-ol / Heating 2: NaH / dimethylformamide 3: N-methylpyrrolidinone / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 21 p. 2697 - 2702
参考文献
Dorff, Peter H.; Garigipati, Ravi S.
Tetrahedron Letters, 2001 , vol. 42, # 15 p. 2771 - 2773
反应条件
1: butan-1-ol / 5 h / 100 °C 2: 40 mg / 3 h / 155 °C / in an evacuated sealed tube View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 25, # 2 p. 303 - 310
参考文献
Hammarstroem, Lars G.J; Smith, David B; Talamas, Francisco X; Labadie, Sharada S; Krauss, Nancy E
Tetrahedron Letters, 2002 , vol. 43, # 45 p. 8071 - 8073
