(4-溴丁基)氨基甲酸苄酯合成路线 (共 6 条)
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Boseggia, Elisa; Gatos, Maddalena; Lucatello, Lorena; Mancin, Fabrizio; Moro, Stefano; Palumbo, Manlio; Sissi, Claudia; Tecilla, Paolo; Tonellato, Umberto; Zagotto, Giuseppe
Journal of the American Chemical Society, 2004 , vol. 126, # 14 p. 4543 - 4549
反应条件
triphenylphosphine in dichloromethane
参考文献
Meiji Seika Kaisha Ltd.
Patent: US6576627 B1, 2003 ;
反应条件
potassium carbonate in 1,4-dioxane; water T=20°C; pH=6 - 8; 1.5 h;
参考文献
Wei; Tomohiro; Kodaka; Okuno
Journal of Organic Chemistry, 2000 , vol. 65, # 26 p. 8979 - 8987
反应条件
triphenylphosphine in tetrahydrofuran; hexane; ethyl acetate
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4604402 A1, 1986 ;
US 4604402 A
Title/Abstract Full Text Show Details
E. R. Squibb and Sons, Inc.
Patent: US4621092 A1, 1986 ;
US 4621092 A
反应条件
1: 91 percent / triethylamine / methanol / 10 h / 20 °C 2: 78 percent / CBr4; PPh3 / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Boseggia, Elisa; Gatos, Maddalena; Lucatello, Lorena; Mancin, Fabrizio; Moro, Stefano; Palumbo, Manlio; Sissi, Claudia; Tecilla, Paolo; Tonellato, Umberto; Zagotto, Giuseppe
Journal of the American Chemical Society, 2004 , vol. 126, # 14 p. 4543 - 4549
反应条件
potassium carbonate in acetonitrile
96 h; Heating;
参考文献
Krivickas, Sara J.; Tamanini, Emiliano; Todd, Matthew H.; Watkinson, Michael
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8280 - 8289