反应条件
1: Et3N / CH2Cl2 / 1 h / 0 °C
2: 10.6 g / LiI / dimethylformamide / 3.5 h / 90 °C
3: 72 percent Turnov. / AgNO2 / diethyl ether / 1.) 0 deg C, 1 d, 2.) r.t., 12 d, in darkness
View Scheme
参考文献
Ko, Soo Sung; Confalone, Pat N.
Tetrahedron, 1985 , vol. 41, # 17 p. 3511 - 3518
