4,4,5,5-四甲基-2-(4-(甲基亚磺酰基)苯基)-1,3,2-二噁硼烷合成路线 （共 3 条）
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=85°C; 4 h;
参考文献
WO2009/70873 A1, ;
Page/Page column 51 ;
WO 2009/070873 A1
反应条件
MoO2Cl2(OPPh3)2; tetra-n-butylammonium nitrate; copper(II) nitrate in acetonitrile T=60°C; 10 h; chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 76, # 13 p. 5240 - 5246
反应条件
1.1: toluene / Reflux 1.2: 2 h / Molecular sieve; Heating 2.1: MoO2Cl2(OPPh3)2; tetra-n-butylammonium nitrate; copper(II) nitrate / acetonitrile / 10 h / 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 13 p. 5240 - 5246
