3-苯基甲基-3,4-二氢-1,4-苯并二氮杂革-2,5-二酮合成路线 （共 5 条）
反应条件
acetic acid
4 h; Heating;
参考文献
Jadidi, Khosrow; Aryan, Reza; Mehrdad, Morteza; Luegger, Thomas; Ekkehardt Hahn; Ng, Seik Weng
Journal of Molecular Structure, 2004 , vol. 692, # 1-3 p. 37 - 42
反应条件
in various solvent(s)
T=250 - 260°C; 10 h;
参考文献
Gupta, Renu; Sirohi, Reenu; Shastri, Sudha; Kishore
Heterocyclic Communications, 2003 , vol. 9, # 4 p. 363 - 366
反应条件
1: 1.) 4,4-dimethylaminopyridine, Et3N, 2.) dicyclohexylcarbodiimide / 1.) CH2Cl2, 0 deg C, 5 min, 2.) CH2Cl2, a) from 0 deg C to RT, 2 h, b) RT, 16 h
2: HCl (gas) / dimethylformamide / 60 °C
View Scheme
参考文献
Akssira; Boumzebra; Kasmi; Dahdouh; Roumestant; Viallefont
Synthetic Communications, 1993 , vol. 23, # 16 p. 2265 - 2272
反应条件
1: 1.) 4,4-dimethylaminopyridine, Et3N, 2.) dicyclohexylcarbodiimide / 1.) CH2Cl2, 0 deg C, 5 min, 2.) CH2Cl2, a) from 0 deg C to RT, 2 h, b) RT, 16 h
2: HCl (gas) / dimethylformamide / 60 °C
View Scheme
参考文献
Akssira; Boumzebra; Kasmi; Dahdouh; Roumestant; Viallefont
Synthetic Communications, 1993 , vol. 23, # 16 p. 2265 - 2272
反应条件
Yield given. Multistep reaction;
参考文献
Mayer, John P.; Zhang, Jingwen; Bjergarde, Kirsten; Lenz, Doug M.; Gaudino, John J.
Tetrahedron Letters, 1996 , vol. 37, # 45 p. 8081 - 8084
