反应条件
n-butyllithium 1) THF, hexane, -50 deg C, 5 min, rt, 1 h; 2) THF, hexane, -20 deg C, 10 min, rt, 1 h; 3) THF, hexane, reflux, 8 h; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mikolajczyk, Marian; Perlikowska, Wieslawa; Omelanczuk, Jan; Cristau, Henri-Jean; Perraud-Darcy, Anne
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9716 - 9722
