氯化铬四氢呋喃复合物 (1:3）合成路线 （共 10 条）
反应条件
zinc in tetrahydrofuran extg. mixt. of CrCl3 and Zn-powder (as catalyst) with abs. THF for 10-15 h in Soxhlet-app., concg. soln.;; pptn.;
参考文献
Journal of Organic Chemistry, , vol. 23, p. 1404 - 1404
反应条件
in tetrahydrofuran byproducts: HCl, hexamethyldisiloxane; Room temperature, dropwise addn. with stirring of trimethylchlorosilane to slurry of metal salt.; Washing (hexane), evapn. at reduced pressure.;
参考文献
Inorganic Chemistry, , vol. 29, p. 1592 - 1593
反应条件
THF in tetrahydrofuran byproducts: acetonitrile;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 29, p. 406 - 407
反应条件
tetrahydrofuran in tetrahydrofuran Soxhlet extn. of solid trichloride with refluxing THF;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1123 - 1126
反应条件
tetrahydrofuran; tetrachloromethane in tetrahydrofuran
参考文献
Journal of Organometallic Chemistry, , vol. 260, # 3 p. C75 - C77
反应条件
in not given 50°C, 12 h;
参考文献
Takahashi, Tamotsu; Liu, Yuanhong; Iesato, Atsushi; Chaki, Shinji; Nakajima, Kiyohiko; Kanno, Ken-Ichiro
Journal of the American Chemical Society, 2005 , vol. 127, # 34 p. 11928 - 11929
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.1.2.6, page 16 - 21
反应条件
in tetrahydrofuran react. at -70°C; heating to 20°C;;
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.1.2.6, page 16 - 21
反应条件
CuCl in tetrahydrofuran
byproducts: KCl; N2 atmosphere; addn. of suspn. of org. compd. in THF to Cr-compd. in THF, addn. of CuCl, stirring (18 h); filtn., removal of THF, distn. (5E-3 Torr, 68-70°C);
参考文献
Thaler, Eric G.; Rypdal, Kristin; Haaland, Arne; Caulton, Kenneth
Inorganic Chemistry, 1989 , vol. 28, p. 2431 - 2434
反应条件
in tetrahydrofuran
react. at -70°C; heating to 20°C;;
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.1.2.6, page 16 - 21
