反应条件
in tetrahydrofuran byproducts: NaCl; Addn. of a Na(Mn(CO)5) soln. to an orange suspn. of (PdPtCl2(μ-dppm)2) (cooling (-78°C), N2, stirring), color turns green-brown on raising temp. to ambient, stirring for 2 h.; Concg. in vac., pptg. with n-hexane, filtering of dark green-brown solid, washing with H2O, extg. with toluene gives orange-red soln. (contg. Mn2(CO)10), and a green solid.;
参考文献
Braunstein, Pierre; Bellefon, Claude de Meric de; Ries, Michel; Fischer, Jean
Organometallics, 1988 , vol. 7, p. 332 - 343
