反应条件
in benzene under N2, soln. of Mn- and Fe-complexes (molar ratio 1:3) in benzene was heated under reflux, at 15 min intervals further portions of Mn-complex were added up to total 2.3 equiv, refluxed for 1 h (total 3 h); volatiles removed in vac., extd. in toluene, extracts chromd. on alumina column, eluted with toluene, blue-black band collected, solvent removed, recrystd. from THF-light petroleum; elem. anal.;
参考文献
Brun, Pascual; Dawkins, Gordon M.; Green, Michael; Mills, Rona M.; Salauen, Jean-Yves; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1357 - 1362
