in toluene under dry Ar atm.; soln. contg. 2,3-diphenylbenzo(g)quinoxaline and PhCH2Mn(CO)5 in dry toluene was refluxed for 14 h; soln. evapd. (vac.); residue dissolved (CH2Cl2); silica gel added; solvent removed (vac.); coated silica gel loaded on the top of a SiO2 column packed in dry n-hexane at 2°C; eluted (CH2Cl2:hexane, 1:4 and 1:1as eluents); solvent removed; elem.;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 21-22 p. 4822 - 4827
in tetrahydrofuran NaMn(CO)5 (1.2 M, 5 mL) added under Ar to 5 mL of 1E-2 M Mn(CO)5(NCCH3)BF4, 0.3 M tetra-n-butylammonium perchlorate added, react. time approx. 30 min;
water in tetrahydrofuran byproducts: H2; hydrolysis at 20°C; products not isolated;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 583 - 588
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 685 - 689
water in tetrahydrofuran byproducts: H2; hydrolysis at 20°C; products not isolated;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 583 - 588
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 685 - 689
water in tetrahydrofuran byproducts: H2; hydrolysis at 20°C; products not isolated;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 583 - 588
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 685 - 689
water in tetrahydrofuran byproducts: H2; hydrolysis at 20°C; products not isolated;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 583 - 588
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 685 - 689
water in tetrahydrofuran byproducts: H2; hydrolysis at 20°C; products not isolated;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 583 - 588
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 685 - 689
