反应条件
in tetrahydrofuran (N2); soln. of Mn compd. added dropwise to soln. of Fe compd. at 22 °C; soln. stirred (48 h); react. mechanism discussed; (N2); solvent removed (vac.); extn. (CH2Cl2); preparative thin-layer chromy. (SiO2, CH2Cl2/hexane 3/7) gave Mn2(CO)10 (a faint yellow band), FeMn(H) compd. (purple band), and FeMn(CH3CO) compd. (orange band);
参考文献
Rosen, Richard P.; Hoke, Jeffrey B.; Whittle, Robert R.; Geoffroy, Gregory L.; Hutchinson, John P.; Zubieta, Jon A.
Organometallics, 1984 , vol. 3, p. 846 - 855
