反应条件
in tetrahydrofuran byproducts: NaCl; Addn. of filtered Na(Mn(CO)5) soln. to a suspn. of Pd2Cl2(μ-dppm)2 (cooling (-78°C), N2, stirring), no react. until warming to 0°C, slow color change (orange to brown-violet).; Filtn. after 4 h, evapn. in vac., addn. of pentane at -20°C, filtn. of brown powder, dissolving in THF, replacing by freshly distd. CH2Cl2, addn. of n-hexane, cooling (-20°C), elem. anal., column chromy. of filtrate yields other complexes.;
参考文献
Organometallics, , vol. 7, p. 332 - 343
