反应条件
sodium cyanoborohydride in tetrahydrofuran byproducts: bis(p-tolyl)silane; under N2; a THF soln. of Mn-complex was added to a suspn. of NaBH3CN in THF at -43°C, mixt. was stirred for 1d at room temp.; evapd. in vacuo, residue was extd. with hexane, filtered through a Celite pad, evapd., flash chromy. (SiO2, toluene/hexane (1/5));
参考文献
Shiozawa, Rie; Tobita, Hiromi; Ogino, Hiroshi
Journal of Organometallic Chemistry, 2002 , vol. 650, # 1-2 p. 91 - 95
