反应条件
potassium in tetrahydrofuran; toluene byproducts: KPF6, MeCN, H2; N2-atmosphere; dropwise addn. of indole in THF to K in cold toluene, refluxing, addn. of Mn-complex in THF, stirring (room temp., 2 d); solvent removal (vac.), addn. of CH2Cl2, filtration, concn. (vac.), chromy. (Al2O3, pentane, then CH2Cl2/pentane=1:5);
参考文献
Ji, Liang-Nian; Kershner, David L.; Rerek, Mark E.; Basolo, Fred
Journal of Organometallic Chemistry, 1985 , vol. 296, p. 83 - 94
