water in hexane
To a soln. of Et3GeLi is added Et2Ge(H)Cl at room temp., mixt. is stirred for 1 h (dry Ar).; detected by GLC;;
参考文献
Pigarev, S. D.; Bravo-Zhivotovskii, D. A.; Kalikhman, I. D.; Vyazankin, N. S.; Voronkov, M. G.
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 29 - 42
water in N,N,N',N',N'',N''-hexamethylphosphoric triamide
To a soln. of Et3GeLi is added Et2Ge(H)Cl at room temp., mixt. is stirred for 1 h (dry Ar).; detected by GLC;;
参考文献
Pigarev, S. D.; Bravo-Zhivotovskii, D. A.; Kalikhman, I. D.; Vyazankin, N. S.; Voronkov, M. G.
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 29 - 42
