3-氨基-n-甲基苯丙酰胺合成路线 （共 3 条）
反应条件
triethylsilane; palladium on activated charcoal in methanol T=20°C; 1 h;
参考文献
LUPIN LIMITED; DAVE, Bhavesh; BANERJEE, Rakesh, Kumar; PHUKAN, Samiron; KHOJE, Abhijit, Datta; HANGARGE, Rajkumar; JADHAV, Jitendra, Sambhaji; PALLE, Venkata, P.; KAMBOJ, Rajender, Kumar
Patent: WO2013/136249 A1, 2013 ;
Location in patent: Page/Page column 53 ;
反应条件
1: N,N-dimethyl-formamide; oxalyl dichloride / toluene / 3 h / |Reflux 2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C 3: triethylsilane; palladium on activated charcoal / methanol / 1 h / 20 °C View Scheme
参考文献
LUPIN LIMITED; DAVE, Bhavesh; BANERJEE, Rakesh, Kumar; PHUKAN, Samiron; KHOJE, Abhijit, Datta; HANGARGE, Rajkumar; JADHAV, Jitendra, Sambhaji; PALLE, Venkata, P.; KAMBOJ, Rajender, Kumar
Patent: WO2013/136249 A1, 2013 ;
反应条件
1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C 2: triethylsilane; palladium on activated charcoal / methanol / 1 h / 20 °C View Scheme
参考文献
LUPIN LIMITED; DAVE, Bhavesh; BANERJEE, Rakesh, Kumar; PHUKAN, Samiron; KHOJE, Abhijit, Datta; HANGARGE, Rajkumar; JADHAV, Jitendra, Sambhaji; PALLE, Venkata, P.; KAMBOJ, Rajender, Kumar
Patent: WO2013/136249 A1, 2013 ;
