反应条件
1: 1.) CuI / 1.) Et2O 2: KN(Me4Si)2 / tetrahydrofuran; dimethylformamide 3: 1.) O3, 2.) (CH3)2S / 1.) MeOH, - 60 deg C 4: CHCl3 / Heating 5: dibal / diethyl ether / -78 - 0 °C 6: TEA, DMAP / CH2Cl2 7: I2 / acetonitrile / 0 °C 8: 13 percent / 1.) AgBF4, 2.) H2O / 26.5 h / 60 °C View Scheme
参考文献
Bartlett; Ting
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2230 - 2240
