2-乙氧基-2,3,3,3-四氟-丙酸乙酯合成路线 (共 7 条)
反应条件
1: hexafluorocyclopropylene oxide; ethanol With silica gel T=20°C; 2: 1,10-phenanthroline in methanol; ethanol 1 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 1 p. 178 - 188
反应条件
a) 1 h, b) 100 deg C, 3 h;
参考文献
Liebigs Annalen der Chemie, , # 2 p. 159 - 162
参考文献
Gazzetta Chimica Italiana, , vol. 98, p. 277 - 289
反应条件
T=225 - 260°C; P=0.01 Torr; 0.666667 h; Product distributionMechanism;
参考文献
Journal of Fluorine Chemistry, , vol. 49, # 1 p. 43 - 66
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4357282 A1, 1982 ;
反应条件
SbF5 in neat (no solvent)
参考文献
England, David C.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4007 - 4008
反应条件
SbF5 in neat (no solvent)
参考文献
England, David C.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4007 - 4008