2-硝基-1-(吡啶-3-基)乙醇合成路线 (共 6 条)
反应条件
acrylic acid methyl ester; triphenylphosphine in ethanol T=20°C; Henry reaction; 1.5 h;
参考文献
Wang, Xiu; Fang, Fan; Zhao, Chen; Tian, Shi-Kai
Tetrahedron Letters, 2008 , vol. 49, # 45 p. 6442 - 6444
反应条件
ammonium acetate T=60°C; Henry reaction; 0.75 h; Ultrasound irradiation;
参考文献
Rodriguez, Jose M.; Dolors Pujol
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2629 - 2632
反应条件
bovine serum albumin in water T=30°C; 16 h;
参考文献
Busto, Eduardo; Gotor-Fernandez, Vicente; Gotor, Vicente
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 236 - 240
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4581178 A1, 1986 ;
反应条件
triethylamine; trifluoroacetic anhydride T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
White, Nicholas A.; Dirocco, Daniel A.; Rovis, Tomislav
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8504 - 8507
反应条件
10 Pd/C; hydrogen in methanol
T=20°C; 12 h;
参考文献
Bhabak, Krishna P.; Arenz, Christoph
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 20 p. 6162 - 6170