6-氯-3-硝基喹啉-4-醇合成路线 （共 4 条）
反应条件
acetic anhydride; potassium carbonate T=90°C; 1 h;
参考文献
KALYPSYS, INC.; BORCHARDT, Allen; DAVIS, Robert; BEAUREGARD, Clay; BECKER, Daniel; GAMACHE, Daniel; NOBLE, Stewart, A.; HELLBERG, Mark, R.; KLIMKO, Peter, G.; ZHIHAI, Qui; PAYNE, Joseph, E.; YANNI, John
Patent: WO2011/112731 A2, 2011 ;
Location in patent: Page/Page column 199-200 ;
WO 2011/112731 A2
反应条件
potassium acetate; acetic anhydride T=120°C; 3 h;
参考文献
Kumar, Sanjay; Vishwakarma, Ram; Mundada, Ramswaroop; Deore, Vijaykumar; Kumar, Pramod; Sharma, Somesh
Patent: US2012/108627 A1, 2012 ;
Location in patent: Page/Page column 16 ;
反应条件
1: aqueous HCl 2: acetic acid anhydride; potassium acetate / 110 °C View Scheme
参考文献
KALYPSYS, INC.; BORCHARDT, Allen; DAVIS, Robert; BEAUREGARD, Clay; BECKER, Daniel; GAMACHE, Daniel; NOBLE, Stewart, A.; HELLBERG, Mark, R.; KLIMKO, Peter, G.; ZHIHAI, Qui; PAYNE, Joseph, E.; YANNI, John
Patent: WO2011/112731 A2, 2011 ;
WO 2011/112731 A2
反应条件
trichlorophosphate
T=120°C; 0.75 h;
参考文献
Kumar, Sanjay; Vishwakarma, Ram; Mundada, Ramswaroop; Deore, Vijaykumar; Kumar, Pramod; Sharma, Somesh
Patent: US2012/108627 A1, 2012 ;
Location in patent: Page/Page column 16 ;
