2-(4-氯苯基)苯并咪唑合成路线 (共 69 条)
反应条件
carbon monoxide; 3 A molecular sieve; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in 1,4-dioxane T=120°C; P=22800 Torr; 3 h;
参考文献
Synlett, , # 1 art. no. U26605ST, p. 109 - 111
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in water; acetonitrile T=150°C; Suzuki coupling; 0.5 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 49, # 47 p. 6667 - 6669
反应条件
bis(benzonitrile)palladium(II) dichloride; 1,1,3,3-tetramethyl-2-thiourea; oxygen; copper diacetate in 1-methyl-pyrrolidin-2-one T=100°C; P=760.051 Torr; 24 h;
参考文献
Chemistry - A European Journal, , vol. 15, # 30 p. 7292 - 7296
反应条件
copper(I) oxide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in water T=100°C; 30 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 76, # 2 p. 716 - 719
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water T=80°C; 0.666667 h;
参考文献
European Journal of Organic Chemistry, , # 29 p. 4926 - 4929
反应条件
1: With copper(l) iodide; K3PO4*3H2O; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=100°C; 3 h; Schlenk techniqueSealed tubeInert atmosphere; 2: With acetic acid in 1,4-dioxane Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Chinese Journal of Chemistry, , vol. 31, # 10 p. 1247 - 1249
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide in neat (no solvent) T=20 - 25°C; 4 h; Green chemistry;
参考文献
Arkivoc, , vol. 2012, # 9 p. 262 - 279
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=120°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 42 p. 7271 - 7275
反应条件
Ru(phen)3(Cl)2; oxygen in dimethyl sulfoxide T=32°C; 36 h; IrradiationSchlenk technique;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 2 p. 502 - 506
Angew. Chem., , vol. 126, # 2 p. 512 - 516,5
反应条件
indium; 2-Bromo-2-nitropropane in methanol; water T=20°C; 5 h;
参考文献
Heterocycles, , vol. 63, # 1 p. 41 - 54