3,4-二甲基-3,4-二苯基己烷合成路线 （共 16 条）
反应条件
[VCl3(tetrahydrofuran)3]; VCl2(N,N,N',N'-tetramethylethylenediamine)2 in tetrahydrofuran various vanadium reagents; Product distribution;
参考文献
Kataoka, Yasutaka; Akiyama, Hiroaki; Makihira, Isamu; Tani, Kazuhide
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 8109 - 8113
反应条件
para-dicyanobenzene in tetrahydrofuran T=22°C; Irradiation;
参考文献
Maslak, Przemyslaw; Chapman Jr., William H.
Tetrahedron, 1990 , vol. 46, # 8 p. 2715 - 2724
反应条件
(t-BuO)2 T=130°C; 20 h;
参考文献
Kratt, Guenter; Beckhaus, Hans-Dieter; Lindner, Hans Joerg; Ruechardt, Christoph
Chemische Berichte, 1983 , vol. 116, # 9 p. 3235 - 3263
反应条件
hydrogen bromide; acetic acid; zinc T=0 - 5°C;
参考文献
Kratt, Guenter; Beckhaus, Hans-Dieter; Lindner, Hans Joerg; Ruechardt, Christoph
Chemische Berichte, 1983 , vol. 116, # 9 p. 3235 - 3263
反应条件
air in acetone 24 h; Ambient temperatureIrradiation; Yield given;
参考文献
Pasternak, Mordechai; Morduchowitz, Abraham
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4275 - 4278
反应条件
1: 92 percent / diethyl ether / 1) 16 h, r.t., 2) 2 h, reflux 2: 12 percent / 40percent HBr, glac. HOAc, Zn / 0 - 5 °C View Scheme
参考文献
Kratt, Guenter; Beckhaus, Hans-Dieter; Lindner, Hans Joerg; Ruechardt, Christoph
Chemische Berichte, 1983 , vol. 116, # 9 p. 3235 - 3263
反应条件
in tetrahydrofuran; methanol T=22°C; Irradiation;
参考文献
Maslak, Przemyslaw; Chapman Jr., William H.
Tetrahedron, 1990 , vol. 46, # 8 p. 2715 - 2724
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2; oxygen 1) THF, 20 deg C, 1 h; 2) THF, reflux, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kataoka, Yasutaka; Akiyama, Hiroaki; Makihira, Isamu; Tani, Kazuhide
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6094 - 6095
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2; oxygen 1) THF, 20 deg C, 1 h; 2) THF, reflux, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kataoka, Yasutaka; Akiyama, Hiroaki; Makihira, Isamu; Tani, Kazuhide
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6094 - 6095
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2 1.) THF; 2.) THF, 25 deg C, 1 h; 3.) THF, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron, 1997 , vol. 53, # 28 p. 9525 - 9540
