3,4-二甲基-3,4-二苯基己烷合成路线 （共 16 条）
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2 1.) THF; 2.) THF, 25 deg C, 1 h; 3.) THF, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron, 1997 , vol. 53, # 28 p. 9525 - 9540
反应条件
air 24 h; Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Pasternak, Mordechai; Morduchowitz, Abraham
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4275 - 4278
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2 1.) THF; 2.) THF, 25 deg C, 1 h; 3.) THF, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron, 1997 , vol. 53, # 28 p. 9525 - 9540
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2; allyl bromide 1.) THF, 20 deg C, 1 h, 2.) 20 deg C, 1 h, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron, 1997 , vol. 53, # 28 p. 9525 - 9540
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2 1.) THF, 20 deg C, 1 h, 2.) 20 deg C, 1 h, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron, 1997 , vol. 53, # 28 p. 9525 - 9540
反应条件
VCl2(N,N,N',N'-tetramethylethylenediamine)2 1.) THF; 2.) THF, 25 deg C, 1 h; 3.) THF, reflux, 12 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kataoka, Yasutaka; Makihira, Isamu; Akiyama, Hiroaki; Tani, Kazuhide
Tetrahedron Letters, 1995 , vol. 36, # 36 p. 6495 - 6498
