双(三苯基膦)氯化铂(II)合成路线 （共 132 条）
反应条件
triphenylphosphine in dichloromethane to soln. of Pt complex was added slight excess of PPh3; after 2 h soln. was evapd. to dryness in vac., residue was washed with hexane; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 186, # 3 p. 411 - 418
反应条件
HCl in ethanol byproducts: o-(NH2)2C6H4*2HCl; N2-atmosphere; addn. of solid Pt-complex to soln. of HCl in EtOH (room temp., room temp.); filtration, washing (EtOH, hexane), drying (vac.);
参考文献
Inorganica Chimica Acta, , vol. 33, p. 161 - 166
反应条件
in neat (no solvent) PtCl2 reacts with molten P(C6H5)3;
参考文献
Chemical Communications, , # 15 p. 1606 - 1607
反应条件
triphenylphosphine in chloroform-d1 cold soln. of PPh3 in CDCl3 added dropwise to soln. of Pt complex in CDCl3 at 213 K; not isolated, monitored by NMR;
参考文献
Inorganic Chemistry, , vol. 22, p. 434 - 438
反应条件
in benzene under N2; a soln. of Ar'PCCl2 (1.6 mmol) in benzene was added to a soln.of Pt-contg. compd. (1.5 mmol) in toluene; the yellow soln. was allowed to stir at room temp.; NMR spectra monitoring; half of the solvent was removed and the solid was isolated.; after 2 wk, the ppt. was sepd. and recrystd. from toluene; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 16 p. 3630 - 3637
反应条件
1: ethanol 2: HCl / ethanol View Scheme
参考文献
Inorganica Chimica Acta, , vol. 33, p. 161 - 166
反应条件
triphenylphosphine in not given N2 atmosphere; filtration;
参考文献
Inorganica Chimica Acta, , vol. 190, p. 119 - 128
反应条件
triphenylphosphine in not given N2 atmosphere; filtration;
参考文献
Inorganica Chimica Acta, , vol. 190, p. 119 - 128
反应条件
triphenylphosphine in not given N2 atmosphere; filtration;
参考文献
Inorganica Chimica Acta, , vol. 190, p. 119 - 128
反应条件
triphenylphosphine in not given N2 atmosphere; filtration;
参考文献
Inorganica Chimica Acta, , vol. 190, p. 119 - 128
