双(三苯基膦)氯化铂(II)合成路线 （共 132 条）
反应条件
in acetone condensing excess ketone onto suspn. of Pt-complex (-196°C), sealing, warming to room temp., shaking for 24 h; removal of volatiles, filtration, washing (Et2O), drying (vac.);
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1906 - 1910
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 348 - 356
反应条件
in benzene byproducts: C6H5CON(C6H5)OCOC6H5; addn. of a benzene soln. of C6H5COCl to the complex under CO2 atm.; 22 h; molar ratio of complex:C6H5COCl = 1:2.2;;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 163 - 168
反应条件
in ethanol; water dil. HCl was added to EtOH suspn. of Pt-compd.; identified by IR and NMR;
参考文献
Polyhedron, , vol. 26, # 16 p. 4737 - 4745
反应条件
in acetone N2-atmosphere; addn. of stoich. amt. of metal chloride to thiocarboxamido-complex (pptn.); filtration, CHCl3 addn., sepn. of soln., concn., pptn. on Et2O addn.;
参考文献
Inorganica Chimica Acta, , vol. 51, p. 263 - 272
反应条件
in methanol; dichloromethane soln. of Pt complex in CH2Cl2 treated dropwise with soln. of ZnCl2 in CH3OH, hydrolized for 36 h;
参考文献
European Journal of Inorganic Chemistry, , # 36 p. 5541 - 5549
反应条件
in dichloromethane r.t., 2 h;
参考文献
Dalton Transactions, , vol. 40, # 34 p. 8664 - 8674
反应条件
in dichloromethane r.t., 2 h;
参考文献
Dalton Transactions, , vol. 40, # 34 p. 8664 - 8674
反应条件
in chloroform stoich., mixed, pptd. for 240 h at 20°C; ppt. filtered, dried (vac.), filtrate evaptd.(vac.), residue washed (ether), IR, NMR;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 9 p. 1759 - 1761
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 30, # 9 p. 2141 - 2143
反应条件
in benzene byproducts: C6H5CON(C6H5)OCOC6H5; addn. of a soln. of C6H5COCl in benzene to the complex under CO2 atm.;;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 163 - 168
