2,6-二氯吡啶-4-甲醇合成路线 （共 14 条）
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=80°C; 12 h;
参考文献
Mello, Jesse V.; Finney, Nathaniel S.
Journal of the American Chemical Society, 2005 , vol. 127, # 29 p. 10124 - 10125
反应条件
sodium tetrahydroborate in ethanol T=80°C; 3 h;
参考文献
Kumar, Rohan J.; Karlsson, Susanne; Streich, Daniel; Jensen, Alice Rolandini; Jaeger, Michael; Becker, Hans-Christian; Bergquist, Jonas; Johansson, Olof; Hammarstroem, Leif
Chemistry - A European Journal, 2010 , vol. 16, # 9 p. 2830 - 2842
反应条件
1: palladium/barium sulfate; xylene / 160 - 170 °C / Hydrogenation 2: 50 percent- aqueous KOH-solution View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>134, p. 177,184
反应条件
1: 72 percent / POCl3 / 24 h / 150 °C 2: 84 percent / H2SO4 / 15 h / Heating 3: 85 percent / NaBH4 / ethanol / 3 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 2 p. 291 - 298
反应条件
sodium tetrahydroborate in ethanol 3 h; Heating;
参考文献
Elhaik, Jerome; Pask, Christopher M.; Kilner, Colin A.; Halcrow, Malcolm A.
Tetrahedron, 2007 , vol. 63, # 2 p. 291 - 298
反应条件
1: SnCl2; HCl; diethyl ether 2: aqueous hydrochloric acid; sodium nitrite View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 52, p. 55,59
反应条件
hydrogenchloride; sodium nitrite
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 52, p. 55,59
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 140, p. 39,43
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 146, p. 88,90
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>134, p. 177,184
反应条件
1: P2O5 / unter vermindertem Druck 2: SnCl2; HCl; diethyl ether 3: aqueous hydrochloric acid; sodium nitrite View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 52, p. 55,59
反应条件
potassium hydroxide; palladium-barium carbonate Hydrogenation;
参考文献
Rabe
Journal fuer Praktische Chemie (Leipzig), 1938 , vol. <2> 151, p. 65,79
