反应条件
1: 1.) TMEDA, BuLi / 1.) ether, hexane, 0 deg C, 2 h, 2.) ether, hexane, room temp., 30 min
2: 1.) ether, -10 deg C, 3 h, 2.) ether, THF, -10 deg C, 1 h
3: 67.1 percent / conc.sulphuric acid / aq. acetic acid / 26 h
4: 1.) BuLi / 1.) ether, hexane, 2.5 h, 2.) ether, hexane, 30 min
View Scheme
参考文献
Townsend, Craig A.; Christensen, Siegfried B.; Davis, Steven G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 839 - 862
