Gmelin Handbook: B: B-Verb.13, 4.7.2.4, page 203 - 209
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McElroy, A. D.; Hunt, R. M.
Patent: US2996539 , 1961 ;
C. A., 1962 , vol. 56, p. 8742
in neat (no solvent)
byproducts: B(OCH3)3; heating equimolar amounts of educts (149-197°C) for 1h, removal of generated B(OCH3)3 in the course of react.;; isomeric mixture after distn. in vac. (isomerization); pure (B(s-C4H9)O)3 after redistn. of the first fraction;;
参考文献
Mc Cusker; Bright
Journal of Organic Chemistry, 1964 , vol. 29, p. 2093
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Gmelin Handbook: B: B-Verb.13, 4.7.2.2, page 189 - 196
