1,1,3,3-四甲氧基丙烷合成路线 （共 127 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Bredereck,H. et al.
Chemische Berichte, 1962 , vol. 95, p. 803 - 809
反应条件
bromine
1.) 40 deg C, 2.) electrolysis, 2.5 F/mol; Yield given. Multistep reaction;
参考文献
Aben, R.W.M.; Hanneman, E.J.M.; Scheeren, J.W.
Synthetic Communications, 1980 , vol. 10, # 11 p. 821 - 826
反应条件
hydrogenchloride; sodium disulfite
参考文献
Saslaw; Waravdekar
Journal of Organic Chemistry, 1957 , vol. 22, p. 843
参考文献
Kikugawa, Kiyomi; Tsukuda, Koichi; Kurechi, Tsutao
Chemical & Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3323 - 3331
反应条件
1: 92 percent / p-TsOH / toluene / Heating
2: 92 percent / BH3*THF / tetrahydrofuran / 96 h / Heating
View Scheme
参考文献
Castro, Peter P.; Tihomirov, Serge; Gutierrez, Carlos G.
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 5179 - 5181
反应条件
thionyl chloride; silica gel in benzene
5 h; Ambient temperature;
参考文献
Cambie, Richard C.; Clark, George R.; Gallagher, Stewart R.; Rutledge, Peter S.; Stone, Martin J.; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 315 - 338
反应条件
hydrogenchloride in chloroform
2 h; Heating;
参考文献
Reddy; Nagarajan
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 5 p. 477 - 478
