1,1,3,3-四甲氧基丙烷合成路线 （共 127 条）
反应条件
acetic acid 2 h; Heating;
参考文献
American Cyanamid Company
Patent: US4847256 A1, 1989 ;
反应条件
hydrogenchloride in ethanol 2 h; Heating;
参考文献
Otteneder, Michael; Plastaras, John P.; Marnett, Lawrence J.
Chemical Research in Toxicology, 2002 , vol. 15, # 3 p. 312 - 318
反应条件
hydrogenchloride in ethanol Heating / reflux;
参考文献
F. HOFFMANN-LA ROCHE AG; GENENTECH, INC.; DO, Steven; HU, Huiyong; KOLESNIKOV, Aleksandr; TSUI, Vickie, H.; WANG, Xiaojing
Patent: WO2014/1377 A1, 2014 ;
Location in patent: Page/Page column 104 ;
反应条件
1: With hydrogenchloride in water T=65°C; 3 h; 2: With sodium hydroxide in water T=15°C; Product distribution / selectivity;
参考文献
NIPPON CARBIDE KOGYO KABUSHIKI KAISHA
Patent: EP1607381 A1, 2005 ;
Location in patent: Page/Page column 8 ;
反应条件
1: With hydrogenchloride in water T=65°C; 3 h; 2: With sodium hydroxide in water T=15°C; Product distribution / selectivity;
参考文献
NIPPON CARBIDE KOGYO KABUSHIKI KAISHA
Patent: EP1607381 A1, 2005 ;
Location in patent: Page/Page column 6-7 ;
反应条件
1: With hydrogenchloride in water T=65°C; 3 h; 2: With sodium hydroxide in water T=15°C; Product distribution / selectivity;
参考文献
NIPPON CARBIDE KOGYO KABUSHIKI KAISHA
Patent: EP1607381 A1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
1: With hydrogenchloride in water T=65°C; 3 h; 2: With sodium hydroxide in water T=15°C; Product distribution / selectivity;
参考文献
NIPPON CARBIDE KOGYO KABUSHIKI KAISHA
Patent: EP1607381 A1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
1: With hydrogenchloride in water T=65°C; 3 h; 2: With sodium hydroxide in water T=15°C; Product distribution / selectivity;
参考文献
NIPPON CARBIDE KOGYO KABUSHIKI KAISHA
Patent: EP1607381 A1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
phosphoric acid T=50°C; 0.5 h;
参考文献
Gueiffier; Fauvelle; Grassy; Dauphin
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 3 p. 765 - 771
反应条件
1: With hydrogenchloride in water 2: With sulfuric acid; nitric acid in water
参考文献
Nishiwaki, Nagatoshi; Ogihara, Takuma; Takami, Toshiko; Tamura, Mina; Ariga, Masahiro
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8382 - 8386
