反应条件
n-butyllithium; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
Ar atmosphere; stirring of Fe-compd. in THF (-70°C, 10 min), addn. of BuLi in hexane, stirring (10 min), cooling (ice bath), addn. ZnI2, stirring (10 min), addn. to soln. of org. compd. and Pd-compd., stirring (3 h, removal of cooling after 2 h); evapn. (vac.), addn. of Et2O, partial evapn., chromy.(silica, hexane/Et2O 70:30);
参考文献
Schottenberger, Herwig; Buchmeiser, Michael; Polin, Johann; Schwarzhans, Karl-Eberhard
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1993 , vol. 48, # 11 p. 1524 - 1532
