反应条件
AgCF3SO3; Li(CH2)3CH3 in tetrahydrofuran; hexane
(under N2); AgCF3SO3 added to RuCl-complex in THF in dark, Li-salt in hexane added to RuPF6-complex in THF, mixed, 18 h, filtered through silicagel column with acetone, solvent removed, ppt. dissolved in CH2Cl2, Fe- complex added; chromy. on silica gel column, eluted with acetone/hexane 1:9, then with acetone/hexane 1:1; elem. anal.;
参考文献
Bruce, Michael I.; Costuas, Karine; Ellis, Ben G.; Halet, Jean-Francois; Low, Paul J.; Moubaraki, Boujemaa; Murray, Keith S.; Ouddai, Nadia; Perkins, Gary J.; Skelton, Brian W.; White, Allan H.
Organometallics, 2007 , vol. 26, # 15 p. 3735 - 3745