反应条件
in toluene
byproducts: LiCl; Ar; Fe compd. (4.32 mmol) in toluene cooled to -60°C, Al compd. (1.01 mmol) added, stirred for 1 h at -60°C and 20 h at room temp., py (2.5 mmol) added at -30°C, stirred for 1 h; evapd., washed (hexane), dried (vac.), recrystd. (toluene-d8, 2 wk, -30°C), elem. anal.;
参考文献
Wrackmeyer, Bernd; Klimkina, Elena V.; Ackermann, Tamara; Milius, Wolfgang
Inorganica Chimica Acta, 2009 , vol. 362, # 11 p. 3941 - 3948
