反应条件
1: 2.) KOH / 1.) room temperature, 1 h, 2.) EtOH, 50 deg C, 1 h 2: 86 percent / Na2WO4-2H2O, aq. H2O2 / 15 h / Ambient temperature; phosphate buffer, pH 5.6 3: 94 percent / Oxone / dioxane; H2O / 2 h / Heating 4: (COCl)2 / CDCl3 / 3 h / Heating 5: 51 percent / CH2Cl2 / 0.5 h / Ambient temperature 6: liquid NH3, Na / tetrahydrofuran / 0.5 h / -78 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 16 p. 5403 - 5412
