3,5-二叔丁基邻苯二酚合成路线 (共 187 条)
反应条件
triethylamine in n-heptane
T=20°C; 24 h;
参考文献
Mukherjee, Soumen; Weyhermueller, Thomas; Bothe, Eberhard; Wieghardt, Karl; Chaudhuri, Phalguni
Dalton Transactions, 2004 , # 22 p. 3842 - 3853
反应条件
in tetrahydrofuran
byproducts: pentamethylcyclopentadiene; (N2); addn. of a soln. of catechol deriv. in THF to a soln. of tin complex in THF at room temp., stirring for 2 h; evapn., washing with Et2O, detected by NMR;
参考文献
Rouzaud; Joudat; Castel; Delpech; Riviere; Gornitzka; Manriquez; Chavez
Journal of Organometallic Chemistry, 2002 , vol. 651, # 1-2 p. 44 - 51
反应条件
oxygen; iron(III) chloride in 1,4-dioxane
T=25°C; P=760 Torr; 24 h; variation of solvents and catalysts; also with quenchers; Product distributionMechanism;
参考文献
Funabiki,T.; Mizoguchi,A.; Sugimoto,T.
Journal of the American Chemical Society, 1986 , vol. 108, p. 2921
反应条件
pyridine; oxygen; tacn; iron(II) chloride
3 h;
参考文献
Lin; Reid; Bugg
Journal of the American Chemical Society, 2001 , vol. 123, # 21 p. 5030 - 5039
反应条件
1: With 1-(2-pyridylmethyl)pyrrolidine-2-carboxylic acid; oxygen; triethylamine in acetonitrile
T=20°C; 12.0333 h;
2: With hydrogenchloride in water
参考文献
Paria, Sayantan; Halder, Partha; Paine, Tapan Kanti
Inorganic Chemistry, 2010 , vol. 49, # 10 p. 4518 - 4523
反应条件
1: With C19H25Cl3FeN5O; sodium tetraphenyl borate; triethylamine in acetonitrile
3652.5 h; Inert atmosphere;
2: With oxygen in acetonitrile
6 h;
参考文献
Wagner, Marit; Limberg, Christian; Tietz, Thomas
Chemistry - A European Journal, 2009 , vol. 15, # 22 p. 5567 - 5576
反应条件
[(1,4,7-triazacyclononane)FeIII(dianionic 3,5-di-tert-butylcatecholate)Cl]; ammonium acetate; oxygen; acetic acid in acetonitrile
pH=5.5; Reagent/catalyst;
参考文献
Chatterjee, Sayanti; Sheet, Debobrata; Paine, Tapan Kanti
Chemical Communications, 2013 , vol. 49, # 87 p. 10251 - 10253
反应条件
silver perchlorate monohydrate; C10H17Cl3FeN3O; oxygen; triethylamine
T=25°C; 4 h;
参考文献
Sundaravel, Karuppasamy; Suresh, Eringathodi; Saminathan, Kolandaivel; Palaniandavar, Mallayan
Dalton Transactions, 2011 , vol. 40, # 32 p. 8092 - 8107
反应条件
bipyridinepyridineiron(III) chloride; oxygen in tetrahydrofuran
T=25°C; 4 h; product yield distribution in function of the reaction time; further products; Product distribution;
参考文献
Funabiki, Takuzo; Mizoguchi, Akira; Sugimoto, Tsunemi; Yoshida, Satohiro
Chemistry Letters, 1983 , p. 917 - 920
反应条件
[Fe((2-pyrid-2-ylethyl)(pyrid-2-ylmethyl)amine)Cl3]; oxygen in water
Kinetics; Reagent/catalystSolvent;
参考文献
Sankaralingam, Muniyandi; Saravanan, Natarajan; Anitha, Natarajan; Suresh, Eringathodi; Palaniandavar, Mallayan
Dalton Transactions, 2014 , vol. 43, # 18 p. 6828 - 6841