3,5-二叔丁基邻苯二酚合成路线 (共 187 条)
反应条件
in benzene byproducts: HCl; in refluxing benzene, HCl removed by distn. off,; anal., 41percent starting germane, 37percent quinone left;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
hydrogenchloride; water in water acid hydrolysis with aq. HCl;
参考文献
Journal of Organometallic Chemistry, , vol. 386, # 2 p. 147 - 156
反应条件
1: sulfuric acid / benzene 2: sulfuric acid / benzene View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 47, # 9 p. 1310 - 1312
反应条件
acetaldehyde in benzene Irradiation; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3657 - 3658
反应条件
1: 81 percent / AcOH / 0.5 h 2: LiAlH4 / ethanol View Scheme
参考文献
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), , vol. 41, # 10.2 p. 2380 - 2384,1868 - 1870
反应条件
in benzene byproducts: HCl; 12 h at 60 ° C in a sealde tube, concn. under reduced pressure; anal.; 38percent starting germane left;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
1: sulfuric acid / benzene / 1 h 2: sulfuric acid / benzene 3: sulfuric acid / benzene View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 47, # 9 p. 1310 - 1312
反应条件
1: sulfuric acid / benzene / 1 h 2: sulfuric acid / benzene / 3 h View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 47, # 9 p. 1310 - 1312
反应条件
in benzene byproducts: HCl; heating in a sealed tube at 80 ° C for 12 h,; concn. (reduced pressure), anal. (IR, H-NMR, MS); 13percent starting germane;
参考文献
Journal of Organometallic Chemistry, , vol. 339, p. 51 - 60
反应条件
C15H16CuN4(1+)*F6P(1-); oxygen; triethylamine in dichloromethane
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 36 p. 6438 - 6442