3,5-二叔丁基邻苯二酚合成路线 (共 187 条)
反应条件
sodium hydroxide in dichloromethane 24 h; Ambient temperature;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
potassium carbonate in ethylene glycol T=120°C; 4 h;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 785 - 788
反应条件
oxygen; iron(III) chloride in 1,4-dioxane T=25°C; P=760 Torr; 24 h; variation of solvents and catalysts; also with quenchers; Product distributionMechanism;
参考文献
Funabiki,T.; Mizoguchi,A.; Sugimoto,T.
Journal of the American Chemical Society, 1986 , vol. 108, p. 2921
反应条件
oxygen; FeCl(DTBC)py2 in tetrahydrofuran; pyridine T=25°C; P=760 Torr; 24 h; var. of catalyst, catechol, conc.; Product distribution;
参考文献
Funabiki, Takuzo; Ishikawa, Michiya; Nagai, Yasutaka; Yorita, Jun; Yoshida, Satohiro
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1951 - 1952
反应条件
pyridine; oxygen; iron(II) chloride in tetrahydrofuran T=25°C; P=760 Torr; also FeCl3, also H2O at var conc.; Product distributionMechanism;
参考文献
Funabiki, Takuzo; Yoneda, Izumi; Ishikawa, Michiya; Ujiie, Mikio; Nagai, Yasutaka; Yoshida, Satohiro
Journal of the Chemical Society, Chemical Communications, 1994 , # 12 p. 1453 - 1454
反应条件
C16H12Cl4FeNO5; oxygen; triethylamine in methanol 48 h;
参考文献
Saberikia, Iraj; Safaei, Elham; Kowsari, Mohammad Hossein; Lee, Yong-Ill; Cotic, Patricia; Bruno, Giuseppe; Rudbari, Hadi Amiri
Journal of Molecular Structure, 2012 , vol. 1029, p. 60 - 67
反应条件
NaOH in toluene byproducts: H2; N2 atmospher; treatment of catechol and NaOH in toluene (stirring, 30 min), dropwise addn. of GaI in toluene (4 h); sepn. of NaI (filtration off, drying), collectin of Ga-complex by evapn. of filtrate;
参考文献
Ozarowski, Andrzej; McGarvey, Bruce R.; El-Hadad, Ahmed; Tian, Zhigang; Tuck, Dennis G.; et al.
Inorganic Chemistry, 1993 , vol. 32, p. 841 - 847
反应条件
C24H36N7Ni2O3S3 in acetonitrile T=25°C; Kinetics; Concentration;
参考文献
Biswas, Apurba; Das, Lakshmi Kanta; Ghosh, Ashutosh
Polyhedron, 2013 , vol. 61, p. 253 - 261
反应条件
sodium hydroxide in dichloromethane 24 h; Ambient temperature;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
periodate form of Amberlyst A26 in chloroform T=20°C; 0.75 h; further reagent;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 509 - 511