6-甲基-2-苯基苯并噻唑合成路线 （共 39 条）
反应条件
1: 54 percent / aq.potassium hydroxide (60 percent) / 7 h / 130 - 150 °C
2: 59 percent / triethylamine / diethyl ether / 0.25 h
3: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: 80 percent / AcOH / ethanol / 20 h / Heating
2: 43 percent / P4S10 / xylene / 24 h / Heating
3: 79 percent / O2; silica / 20 h / 100 °C
View Scheme
参考文献
Charrier, Jean-Damien; Landreau, Cyrille; Deniaud, David; Reliquet, Francoise; Reliquet, Alain; Meslin, Jean Claude
Tetrahedron, 2001 , vol. 57, # 19 p. 4195 - 4202
反应条件
1: 80 percent / AcOH / ethanol / 20 h / Heating
2: 43 percent / P4S10 / xylene / 24 h / Heating
3: 79 percent / O2; silica / 20 h / 100 °C
View Scheme
参考文献
Charrier, Jean-Damien; Landreau, Cyrille; Deniaud, David; Reliquet, Francoise; Reliquet, Alain; Meslin, Jean Claude
Tetrahedron, 2001 , vol. 57, # 19 p. 4195 - 4202
反应条件
1: 43 percent / P4S10 / xylene / 24 h / Heating
2: 79 percent / O2; silica / 20 h / 100 °C
View Scheme
参考文献
Charrier, Jean-Damien; Landreau, Cyrille; Deniaud, David; Reliquet, Francoise; Reliquet, Alain; Meslin, Jean Claude
Tetrahedron, 2001 , vol. 57, # 19 p. 4195 - 4202
反应条件
1.1: tetrahydrofuran / 12 h / 20 °C
2.1: potassium ethylxanthate; copper diacetate / N,N-dimethyl-formamide / 15 h / 80 °C / |Inert atmosphere
2.2: 8 h / 20 °C
View Scheme
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
反应条件
1: 19 percent / potassium hydroxide / H2O; tetrahydrofuran / 1.5 h
2: 86 percent / potassium hydroxide / methanol / 24 h
3: 65 percent / triethylamine / acetonitrile / standing overnight
4: potassium hydroxide / ethanol / 1.5 h / Heating
5: H2O / Schotten-Baumann
6: potassium hydroxide / ethanol / 3 h / 180 °C / sealed tube
7: 59 percent / triethylamine / diethyl ether / 0.25 h
8: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: 59 percent / triethylamine / diethyl ether / 0.25 h
2: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: 65 percent / triethylamine / acetonitrile / standing overnight
2: potassium hydroxide / ethanol / 1.5 h / Heating
3: H2O / Schotten-Baumann
4: potassium hydroxide / ethanol / 3 h / 180 °C / sealed tube
5: 59 percent / triethylamine / diethyl ether / 0.25 h
6: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: potassium hydroxide / ethanol / 3 h / 180 °C / sealed tube
2: 59 percent / triethylamine / diethyl ether / 0.25 h
3: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
反应条件
1: potassium hydroxide / ethanol / 1.5 h / Heating
2: H2O / Schotten-Baumann
3: potassium hydroxide / ethanol / 3 h / 180 °C / sealed tube
4: 59 percent / triethylamine / diethyl ether / 0.25 h
5: 80 percent / triethylamine / diethyl ether / standing overnight
View Scheme
参考文献
Drozd, V.N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 317 - 326
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 2 p. 355 - 365
