1-(5-溴-2-硝基苯基)乙醇合成路线 (共 3 条)
反应条件
sodium tetrahydroborate in diethyl ether T=0 - 20°C; 2 h;
参考文献
Samsung Electronics Co., Ltd.
Patent: US7566773 B2, 2009 ;
Location in patent: Page/Page column 13 ;
反应条件
1: in tetrahydrofuran T=-78°C; 0.25 h; 2: With water in tetrahydrofuran
参考文献
SmithKline Beecham Corporation
Patent: US2008/96921 A1, 2008 ;
Location in patent: Page/Page column 83-84 ;
反应条件
1: With Jone's reagent in acetone
T=0°C; 0.166667 h;
2: With water; sodium hydrogencarbonate in isopropyl alcohol; acetone
参考文献
SmithKline Beecham Corporation
Patent: US2008/96921 A1, 2008 ;
Location in patent: Page/Page column 84 ;