1-环丁基丁烷-1,3-二酮合成路线 (共 3 条)
反应条件
1: With potassium tert-butylate in tert-butyl methyl ether T=0°C; 2 h; 2: With hydrogenchloride; water in tert-butyl methyl ether
参考文献
US2008/96950 A1, ;
Page/Page column 18 ;
US 20080096950 A1
反应条件
sodium amide in diethyl ether 4 h; Inert atmosphere;
参考文献
WO2013/173441 A2, ;
Page/Page column 56; 57 ;
反应条件
1: sulfuric acid / |Reflux 2: sodium amide / diethyl ether / 4 h / |Inert atmosphere View Scheme